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1.
Materials (Basel) ; 16(24)2023 Dec 11.
Artigo em Inglês | MEDLINE | ID: mdl-38138739

RESUMO

Auxetic structures, renowned for their unique lateral expansion under longitudinal strain, have attracted significant research interest due to their extraordinary mechanical characteristics, such as enhanced toughness and shear resistance. This study provides a systematic exploration of these structures, constructed from rigid rotating square or rectangular unit cells. Incremental alterations were applied to key geometrical parameters, including the angle (θ) between connected units, the side length (a), the side width (b) of the rotating rigid unit, and the overlap distance (t). This resulted in a broad tunable range of negative Poisson's ratio values from -0.43 to -1.78. Through comprehensive three-dimensional finite-element analyses, the intricate relationships between the geometric variables and the resulting bulk Poisson's ratio of the modeled auxetic structure were elucidated. This analysis affirmed the auxetic behavior of all investigated samples, characterized by lateral expansion under tensile force. The study also revealed potential stress concentration points at interconnections between rotating units, which could impact the material's performance under high load conditions. A detailed investigation of various geometrical parameters yielded fifty unique samples, enabling in-depth observation of the impacts of geometric modifications on the overall behavior of the structures. Notably, an increase in the side width significantly enhanced the Poisson's ratio, while an increase in the overlap distance notably reduced it. The greatest observable change in the Poisson's ratio was a remarkable 202.8%, emphasizing the profound influence of geometric parameter manipulation. A cascaded forward propagation-backpropagation neural network model was deployed to determine the Poisson's ratio for auxetic structures, based on the geometric parameters and material properties of the structure. The model's architecture consisted of five layers with varying numbers of neurons. The model's validity was affirmed by comparing its predictions with FEA simulations, with the maximum error observed in the predicted Poisson's ratio being 8.62%.

2.
Materials (Basel) ; 16(11)2023 May 30.
Artigo em Inglês | MEDLINE | ID: mdl-37297219

RESUMO

The friction stir welding (FSW) process was recently developed to overcome the difficulty of welding non-ferrous alloys and steels. In this study, dissimilar butt joints between 6061-T6 aluminum alloy and AISI 316 stainless steel were welded by FSW using different processing parameters. The grain structure and precipitates at the different welded zones of the various joints were intensively characterized by the electron backscattering diffraction technique (EBSD). Subsequently, the FSWed joints were tensile tested to examine the mechanical strength compared with that of the base metals. The micro-indentation hardness measurements were conducted to reveal the mechanical responses of the different zones in the joint. The EBSD results of the microstructural evolution showed that a significant continuous dynamic recrystallization (CDRX) occurred in the stir zone (SZ) of the Al side, which was mainly composed of the weak metal, Al, and fragmentations of the steel. However, the steel underwent severe deformation and discontinuous dynamic recrystallization (DDRX). The FSW rotation speed increased the ultimate tensile strength (UTS) from 126 MPa at a rotation speed of 300 RPM to 162 MPa at a rotation speed of 500 RPM. The tensile failure occurred at the SZ on the Al side for all specimens. The impact of the microstructure change in the FSW zones was significantly pronounced in the micro-indentation hardness measurements. This was presumably attributed to the promotion of various strengthening mechanisms, such as grain refinement due to DRX (CDRX or DDRX), the appearance of intermetallic compounds, and strain hardening. The aluminum side underwent recrystallization as a result of the heat input in the SZ, but the stainless steel side did not experience recrystallization due to inadequate heat input, resulting in grain deformation instead.

3.
Materials (Basel) ; 16(6)2023 Mar 22.
Artigo em Inglês | MEDLINE | ID: mdl-36984403

RESUMO

In the present study, the hydrogen embrittlement (HE) susceptibility of an additively manufactured (AM) 316L stainless steel (SS) was investigated. The materials were fabricated in the form of a lattice auxetic structure with three different strut thicknesses, 0.6, 1, and 1.4 mm, by the laser powder bed fusion technique at a volumetric energy of 70 J·mm-3. The effect of H charging on the strength and ductility of the lattice structures was evaluated by conducting tensile testing of the H-charged specimens at a slow strain rate of 4 × 10-5 s-1. Hydrogen was introduced to the specimens via electrochemical charging in an NaOH aqueous solution for 24 h at 80 °C before the tensile testing. The microstructure evolution of the H-charged materials was studied using the electron backscattered diffraction (EBSD) technique. The study revealed that the auxetic structures of the AM 316L-SS exhibited a slight reduction in mechanical properties after H charging. The tensile strength was slightly decreased regardless of the thickness. However, the ductility was significantly reduced with increasing thickness. For instance, the strength and uniform elongation of the auxetic structure of the 0.6 mm thick strut were 340 MPa and 17.4% before H charging, and 320 MPa and 16.7% after H charging, respectively. The corresponding values of the counterpart's 1.4 mm thick strut were 550 MPa and 29% before H charging, and 523 MPa and 23.9% after H charging, respectively. The fractography of the fracture surfaces showed the impact of H charging, as cleavage fracture was a striking feature in H-charged materials. Furthermore, the mechanical twins were enhanced during tensile straining of the H-charged high-thickness material.

4.
Materials (Basel) ; 15(10)2022 May 13.
Artigo em Inglês | MEDLINE | ID: mdl-35629543

RESUMO

Severe shot peening (SSP) was used on additive manufactured 316L by laser powder bed fusion. The effect of the post processing on the surface features of the material was analyzed through residual stress measurements, tensile testing, hardness-depth profiles, and fatigue testing by flexural bending. The results showed that SSP can be utilized to form residual stresses up to -400 MPa 200 µm below the surface. At the same time, a clear improvement on the surface hardness was achieved from 275 HV to near 650 HV. These together resulted in a clear improvement on material strength which was recorded at 10% improvement in ultimate tensile strength. Most significantly, the fatigue limit of the material was tripled from 200 MPa to over 600 MPa and the overall fatigue strength raised similarly from a low to high cycle regime.

5.
Materials (Basel) ; 14(19)2021 Sep 26.
Artigo em Inglês | MEDLINE | ID: mdl-34639977

RESUMO

In this study, ultra-high-strength steels, namely, cold-hardened austenitic stainless steel AISI 301 and martensitic abrasion-resistant steel AR600, as base metals (BMs) were butt-welded using a disk laser to evaluate the microstructure, mechanical properties, and effect of post-weld heat treatment (PWHT) at 250 °C of the dissimilar joints. The welding processes were conducted at different energy inputs (EIs; 50-320 J/mm). The microstructural evolution of the fusion zones (FZ) in the welded joints was examined using electron backscattering diffraction (EBSD) and laser scanning confocal microscopy. The hardness profiles across the weldments and tensile properties of the as-welded joints and the corresponding PWHT joints were measured using a microhardness tester and universal material testing equipment. The EBSD results showed that the microstructures of the welded joints were relatively similar since the microstructure of the FZ was composed of a lath martensite matrix with a small fraction of austenite. The welded structure exhibited significantly higher microhardness at the lower EIs of 50 and 100 J/mm (640 HV). However, tempered martensite was promoted at the high EI of 320 J/mm, significantly reducing the hardness of the FZ to 520 HV. The mechanical tensile properties were considerably affected by the EI of the as-welded joints. Moreover, the PWHT enhanced the tensile properties by increasing the deformation capacity due to promoting the tempered martensite in the FZ.

6.
Materials (Basel) ; 14(19)2021 Oct 04.
Artigo em Inglês | MEDLINE | ID: mdl-34640206

RESUMO

Additive manufacturing (AM) is an emerging fabrication technology that offers unprecedented potential for manufacturing end-to-end complex shape customized products. However, building products with high performance by AM presents a technological challenge. Inadequate processing parameters, fabrication environment or changes in powder properties may lead to high defect density in the part and poor mechanical properties. Microstructure, defect structure, and mechanical properties of AISI 316L stainless steel pieces, additively manufactured by the laser powder bed fusion method using three different volume energy densities (VEDs), were investigated and compared with those of a commercial wrought AISI 316L sheet. Scanning and transmission electron microscopies were employed for characterization of grain and defect structures, and mechanical properties were determined by tensile testing. It was found that the number of defects such as pores and lack of fusion in AM specimens did not affect the strength, but they impaired the post-uniform elongation, more significantly when processed with the low VED. Twinning was found to be an active deformation mechanism in the medium and high VED specimens and in the commercially wrought material in the later stage of straining, but it was suppressed in the low VED specimens presumably because the presence of large voids limited the strain attained in the matrix.

7.
Opt Lett ; 44(10): 2574-2577, 2019 May 15.
Artigo em Inglês | MEDLINE | ID: mdl-31090735

RESUMO

Testing and characterization techniques intended for traditional electronics production are rarely compatible with modern large-area, thin film electronics manufacturing processes such as roll-to-roll fabrication. Online quality monitoring of conductive thin films is necessary for upscaling and maintaining high-yield production. Thermography has already shown its usefulness in these kinds of applications, but has suffered from the lack of proper non-contact electrical heating. Now a fully contactless quality inspection technique based on thermal imaging and induction heating is implemented and evaluated. This approach is capable of discovering defected areas and estimating conductivity degradation online with full coverage over conductive thin films.

8.
J Mater Sci ; 53(24): 16585-16597, 2018.
Artigo em Inglês | MEDLINE | ID: mdl-30393393

RESUMO

High-pressure torsion (HPT) processing was applied to cast pure magnesium, and the effects of the deformation on the microstructure, hardness, tensile properties and corrosion resistance were evaluated. The microstructures of the processed samples were examined by electron backscatter diffraction, and the mechanical properties were determined by Vickers hardness and tensile testing. The corrosion resistance was studied using electrochemical impedance spectroscopy in a 3.5% NaCl solution. The results show that HPT processing effectively refines the grain size of Mg from millimeters in the cast structure to a few micrometers after processing and also creates a basal texture on the surface. It was found that one or five turns of HPT produced no significant difference in the grain size of the processed Mg and the hardness was a maximum after one turn due to recovery in some grains. Measurements showed that the yield strength of the cast Mg increased by about seven times whereas the corrosion resistance was not significantly affected by the HPT processing.

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